1NOL

OXYGENATED HEMOCYANIN (SUBUNIT TYPE II)

Experimental procedure

Temperature [K]	293
Detector technology	DIFFRACTOMETER
Detector	ENRAF-NONIUS FAST
Wavelength(s)	1.5418
Spacegroup name	R 3 2
Unit cell lengths	117.002, 117.002, 117.002
Unit cell angles	60.02, 60.02, 60.02

Refinement procedure

Resolution	8.000 - 2.400
R-factor	0.181
Rwork	0.181
RMSD bond length	0.018
RMSD bond angle	3.400
Data reduction software	MADNES
Phasing software	X-PLOR (2.1)
Refinement software	X-PLOR (2.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	33.800
High resolution limit [Å]	2.400
Rmerge	0.052
Number of reflections	24861
Completeness [%]	83.7
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *