1NJR

Crystal structure of yeast ymx7, an ADP-ribose-1''-monophosphatase

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X25
Synchrotron site	NSLS
Beamline	X25
Temperature [K]	100
Detector technology	CCD
Collection date	2002-09-24
Detector	BRANDEIS - B4
Wavelength(s)	0.979
Spacegroup name	C 1 2 1
Unit cell lengths	107.694, 38.149, 64.736
Unit cell angles	90.00, 112.21, 90.00

Refinement procedure

Resolution	50.000 - 1.900
Rwork	0.206
R-free	0.23000
Structure solution method	MAD
RMSD bond length	0.010
RMSD bond angle	1.201
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.970
High resolution limit [Å]	1.900	1.900
Rmerge	0.117	0.266
Number of reflections	18988
<I/σ(I)>	18.3
Completeness [%]	97.8	84
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5	293	PEG 6000, Citric acid, Xylitol, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K