1NIH
Structure of deoxy-quaternary haemoglobin with liganded beta subunits
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 63.180, 82.260, 55.060 |
| Unit cell angles | 90.00, 98.42, 90.00 |
Refinement procedure
| Resolution | ? - 2.600 |
| Rwork | 0.214 |
| RMSD bond length | 0.030 |
| Refinement software | EREF |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.600 * |
| Rmerge | 0.058 * |
| Total number of observations | 34793 * |
| Number of reflections | 17218 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.8 * | crystals were grown under a CO atomosphere. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | PEG1000 | 16.9 (%(w/v)) | |
| 2 | 1 | 1 | inositol hexaphosphate | 1 (mM) | |
| 3 | 1 | 1 | potassium phosphate | 5.5 (mM) | |
| 4 | 1 | 1 | hybrid haemoglobin | 0.5 (mM) |
