1NI1
Imidazole and cyanophenyl farnesyl transferase inhibitors
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2000-02-25 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.00000 |
| Spacegroup name | P 61 |
| Unit cell lengths | 170.096, 170.096, 69.286 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.850 - 2.300 |
| Rwork | 0.264 |
| R-free | 0.32700 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond angle | 0.008 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.850 | 2.440 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Number of reflections | 45916 | |
| Completeness [%] | 90.1 | 61.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
