1NES

STRUCTURE OF THE PRODUCT COMPLEX OF ACETYL-ALA-PRO-ALA WITH PORCINE PANCREATIC ELASTASE AT 1.65 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	51.400, 58.200, 75.400
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 1.650
Rwork	0.184
Refinement software	EREF

Data quality characteristics

	Overall
High resolution limit [Å]	1.650 *
Number of reflections	20665 *
Completeness [%]	72.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	PPEase	5 (%(w/v))
2	1	1	sodium acetate	0.1 (M)
3	1	1	sodium azide	0.02 (%(w/v))
4	1	2	sodium sulphate	0.1 (M)