1NAR

CRYSTAL STRUCTURE OF NARBONIN REFINED AT 1.8 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	46.900, 75.500, 50.900
Unit cell angles	90.00, 120.50, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.159
RMSD bond length	0.015
RMSD bond angle	0.046
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.056 *	0.078 *
Total number of observations	124224 *
Number of reflections	27227 *
Completeness [%]	95.5 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	9.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	50 (mg/ml)
2	1	drop	Tris-HCl	0.1 (M)
3	1	drop		0.45 (M)
4	1	reservoir	Tris-HCl	0.1 (M)	(pH 7.2)
5	1	reservoir	acetic acid		some drops