1NAH
UDP-GALACTOSE 4-EPIMERASE FROM ESCHERICHIA COLI, REDUCED
Experimental procedure
Spacegroup name | P 32 2 1 |
Unit cell lengths | 83.500, 83.500, 108.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 1.800 |
R-factor | 0.165 * |
Rwork | 0.165 |
RMSD bond length | 0.015 |
RMSD bond angle | 14.900 * |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 * | |
High resolution limit [Å] | 1.800 * | 1.800 * |
Rmerge | 0.021 * | 0.076 * |
Total number of observations | 72653 * | |
Number of reflections | 39891 | 7216 * |
Completeness [%] | 97.0 | 94 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | enzyme | 60 (mg/ml) | |
2 | 1 | drop | UDP | 5 (mM) | |
3 | 1 | drop | PEG8000 | 15 (%) | |
4 | 1 | drop | 500 (mM) | ||
5 | 1 | drop | HEPES | 50 (mM) | |
6 | 1 | reservoir | PEG | 15 (%) |