1MVM
MVM(STRAIN I), COMPLEX(VIRAL COAT/DNA), VP2, PH=7.5, T=4 DEGREES C
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 277 |
| Detector technology | IMAGE PLATE |
| Collection date | 1993-01 |
| Detector | FUJI |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 448.700, 416.700, 305.300 |
| Unit cell angles | 90.00, 95.80, 90.00 |
Refinement procedure
| Resolution | ? - 3.500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | CANINE PARVOVIRUS (MONOCLINIC FORM) |
| Data reduction software | PURDUE (DATA PROCESSING PACKAGE) |
| Data scaling software | PURDUE (DATA PROCESSING PACKAGE) |
| Phasing software | PURDUE (DATA PROCESSING PACKAGE) |
| Refinement software | NONE |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 3.500 |
| Rmerge | 0.155 |
| Total number of observations | 933857 * |
| Number of reflections | 551094 * |
| Completeness [%] | 64.6 * |
| Redundancy | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.5 | pH 7.50 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG8000 | 0.75 (%(w/v)) | |
| 2 | 1 | reservoir | 8 (mM) | ||
| 3 | 1 | reservoir | Tris-HCl | 10 (mM) | |
| 4 | 1 | drop | PEG8000 | 0.375 (%(w/v)) | |
| 5 | 1 | drop | 4 (mM) | ||
| 6 | 1 | drop | Tris-HCl | 10 (mM) | |
| 7 | 1 | drop | virus | 5 (mg/ml) |
