1MTV
FACTOR XA SPECIFIC INHIBITOR IN COMPLEX WITH BOVINE TRYPSIN
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 287 |
| Detector technology | AREA DETECTOR |
| Collection date | 1995-03 |
| Detector | SIEMENS |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 54.800, 54.800, 109.700 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 1.900 |
| R-factor | 0.169 |
| Rwork | 0.169 |
| Structure solution method | DIFFERENCE FOURIER |
| RMSD bond length | 0.008 |
| RMSD bond angle | 25.200 * |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.037 | 0.140 |
| Total number of observations | 26673 * | |
| Number of reflections | 14594 | |
| <I/σ(I)> | 12 | 3 |
| Completeness [%] | 93.1 | 82.3 |
| Redundancy | 1.8 | 1.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 8 * | 0.1M AMMONIUM SULFATE, PH 7.0, 20% PEG 8000 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 0.1 (M) | |
| 2 | 1 | reservoir | PEG8000 | 20 (%) |
