1MPO

MALTOPORIN MALTOHEXAOSE COMPLEX

Experimental procedure

Source type	SYNCHROTRON
Source details	MPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron site	MPG/DESY, HAMBURG
Beamline	BW6
Temperature [K]	293
Detector technology	IMAGE PLATE
Collection date	1994-11-02
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
Unit cell lengths	129.800, 211.700, 218.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.800
R-factor	0.23
Rwork	0.230
R-free	0.25100
RMSD bond length	0.020
RMSD bond angle	28.400 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.800	2.800 *
Rmerge	0.083	0.370 *
Number of reflections	68475
Completeness [%]	94.3	95.3 *
Redundancy	3	3.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7		pH 7.

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	beta-D-decylmaltoside	0.4 (%(w/w))
2	1	1	HEPES	20 (mM)
3	1	1		0.1 (M)
4	1	1	PEG2000	11.0-12.5 (%(w/w))