1MPJ

X-RAY CRYSTALLOGRAPHIC STUDIES ON HEXAMERIC INSULINS IN THE PRESENCE OF HELIX-STABILIZING AGENTS, THIOCYANATE, METHYLPARABEN AND PHENOL

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	80.700, 80.700, 37.800
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.300
R-factor	0.1893
RMSD bond length	0.016
RMSD bond angle	0.048
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	7.170 *
High resolution limit [Å]	2.300 *	2.300 *
Rmerge	0.030 *
Total number of observations	8990 *
Number of reflections	4058 *
Completeness [%]	96.9 *	84.8 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *	8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	hydrochrolic acid	0.02 (M)