1MNP
MANGANESE PEROXIDASE
Experimental procedure
| Collection date | 1993-06-18 |
| Detector | SIEMENS |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 163.240, 45.970, 53.715 |
| Unit cell angles | 90.00, 97.16, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.060 * |
| R-factor | 0.2 |
| Rwork | 0.200 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.370 |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.060 * |
| Rmerge | 0.062 * |
| Total number of observations | 139176 * |
| Number of reflections | 27040 |
| Completeness [%] | 99.0 |
| Redundancy | 5.15 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG8000 | 30 (%) | |
| 2 | 1 | drop | ammonium sulfate | 0.20 (M) | |
| 3 | 1 | drop | sodium cacodylate | 0.1 (M) | |
| 4 | 1 | drop | protein | 0.005 to 0.010ml |
