1MDF
CRYSTAL STRUCTURE OF DhbE IN ABSENCE OF SUBSTRATE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Collection date | 2001-03-10 |
Spacegroup name | P 31 |
Unit cell lengths | 65.450, 65.450, 106.720 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 100.000 - 2.500 |
Rwork | 0.204 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1md9 |
RMSD bond length | 0.006 * |
RMSD bond angle | 1.350 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | |
High resolution limit [Å] | 2.500 | |
Rmerge | 0.088 * | 0.318 * |
Total number of observations | 42630 * | |
Number of reflections | 17099 * | |
Completeness [%] | 96.5 * | 92.4 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 8.6 * | 18 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 8 (mg/ml) | |
2 | 1 | reservoir | PEG4000 | 30 (%) | |
3 | 1 | reservoir | Tris-HCl | 0.1 (M) | |
4 | 1 | reservoir | 0.2 (M) | pH8.6 |