1M51

PEPCK complex with a GTP-competitive inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	110
Detector technology	IMAGE PLATE
Collection date	1998-09-29
Detector	MARRESEARCH
Wavelength(s)	1.5418
Spacegroup name	P 1
Unit cell lengths	45.407, 61.067, 62.007
Unit cell angles	88.91, 70.21, 72.62

Refinement procedure

Resolution	50.000 - 2.250
R-factor	0.18087
Rwork	0.178
R-free	0.23665
Structure solution method	rigid-body refinement
RMSD bond length	0.012
RMSD bond angle	1.237
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.330
High resolution limit [Å]	2.250	2.250
Number of reflections	26567
<I/σ(I)>	29.6
Completeness [%]	94.1	88.2
Redundancy	1.9	1.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *			VAPOR DIFFUSION