1M51
PEPCK complex with a GTP-competitive inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 110 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-09-29 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 |
| Unit cell lengths | 45.407, 61.067, 62.007 |
| Unit cell angles | 88.91, 70.21, 72.62 |
Refinement procedure
| Resolution | 50.000 - 2.250 |
| R-factor | 0.18087 |
| Rwork | 0.178 |
| R-free | 0.23665 |
| Structure solution method | rigid-body refinement |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.237 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.330 |
| High resolution limit [Å] | 2.250 | 2.250 |
| Number of reflections | 26567 | |
| <I/σ(I)> | 29.6 | |
| Completeness [%] | 94.1 | 88.2 |
| Redundancy | 1.9 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | VAPOR DIFFUSION |
