1LYN

CRYSTAL STRUCTURE AND SUBUNIT DYNAMICS OF THE LYSIN DIMER: EGG ENVELOPES DISSOCIATE DIMERS, THE MONOMER IS THE ACTIVE SPECIES

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1993
Detector	MARRESEARCH
Wavelength(s)	1.5418
Spacegroup name	P 2 2 21
Unit cell lengths	51.200, 47.000, 123.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.750
R-factor	0.233
Rwork	0.233
RMSD bond length	0.023
RMSD bond angle	4.050
Data reduction software	MARXDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.600 *	2.600 *
Rmerge	0.054	0.152 *
Number of reflections	24754
Completeness [%]	93.6
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *