1LXT
STRUCTURE OF PHOSPHOTRANSFERASE PHOSPHOGLUCOMUTASE FROM RABBIT
Experimental procedure
| Temperature [K] | 300 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-11 |
| Detector | XUONG-HAMLIN MULTIWIRE |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 174.420, 174.420, 101.120 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.700 |
| R-factor | 0.201 |
| Rwork | 0.201 |
| R-free | 0.26000 |
| Structure solution method | MODEL REFINEMENT |
| Starting model (for MR) | 3pmg |
| RMSD bond length | 0.017 |
| RMSD bond angle | 24.600 * |
| Data reduction software | XDS |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.800 |
| High resolution limit [Å] | 2.570 | 2.700 |
| Rmerge | 0.150 | |
| Number of reflections | 45619 | |
| Completeness [%] | 97.0 | 60 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG600 | 55 (%) | |
| 2 | 1 | reservoir | MES | 10 (mM) | |
| 3 | 1 | reservoir | 1 (mM) |
