1LXA

UDP N-ACETYLGLUCOSAMINE ACYLTRANSFERASE

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1995
Detector	SIEMENS
Wavelength(s)	1.5418
Spacegroup name	P 21 3
Unit cell lengths	99.000, 99.000, 99.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	99.000 - 2.600
Rwork	0.184
RMSD bond length	0.012
RMSD bond angle	2.400
Data reduction software	XDS
Phasing software	X-PLOR
Refinement software	TNT (5E)

Data quality characteristics

	Overall
Low resolution limit [Å]	99.000
High resolution limit [Å]	2.600
Rmerge	0.080
Total number of observations	79727 *
Number of reflections	8868
Completeness [%]	87.0
Redundancy	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium phosphate	1.9 (M)	or potassium phosphate
2	1	reservoir	dimethylsulfoxide	15-20 (%(v/v))