1LPE

THREE-DIMENSIONAL STRUCTURE OF THE LDL RECEPTOR-BINDING DOMAIN OF HUMAN APOLIPOPROTEIN E

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	40.650, 53.960, 85.430
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.500 *
Rwork	0.175
RMSD bond length	0.017
RMSD bond angle	3.200
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.054 *
Total number of observations	17129 *
Number of reflections	6899 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	reservior	PEG400	15 (%)
3	1	reservoir	sodium acetate-acid	20 (mM)
4	1	reservoir	beta-n-octylglucopyranoside	0.2 (%)
5	1	reservoir	beta-mercaptoethanol	0.1 (%)