Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 258 |
| Detector technology | AREA DETECTOR |
| Detector | UCSD MARK II |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.220, 68.720, 57.030 |
| Unit cell angles | 90.00, 92.20, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.800 |
| R-factor | 0.189 |
| Rwork | 0.189 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 8.000 * |
| High resolution limit [Å] | 1.800 |
| Rmerge | 0.052 * |
| Total number of observations | 101275 * |
| Number of reflections | 28193 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7 | 20 * | taken from Jordan, S.R. et al.(1985). Science, 230, 1383-1385. * |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | PEG 400 | ||
| 3 | 1 | 1 | BIS-TRIS-PROPANE_HCL | ||
| 4 | 1 | 2 | WATER | ||
| 5 | 1 | 2 | PEG 400 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG400 | 20 (%(v/v)) | |
| 2 | 1 | reservoir | PEG400 | 20 (%(v/v)) |
