1LIE

X-RAY CRYSTALLOGRAPHIC STRUCTURES OF ADIPOCYTE LIPID BINDING PROTEIN COMPLEXED WITH PALMITATE AND HEXADECANESULFONIC ACID. PROPERTIES OF CAVITY BINDING SITES

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	119.540, 37.860, 28.570
Unit cell angles	90.00, 92.66, 90.00

Refinement procedure

Resolution	10.000 - 1.600
R-factor	0.198
Rwork	0.198
R-free	0.23900
RMSD bond length	0.021
RMSD bond angle	1.650
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.600 *
Rmerge	0.036 *
Total number of observations	73035 *
Number of reflections	16514 *
Completeness [%]	96.4 *
Redundancy	5.3 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *