1LHT

LOGGERHEAD SEA TURTLE MYOGLOBIN (CYANO-MET)

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1994-10-01
Detector	RIGAKU RAXIS
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	37.570, 61.270, 75.290
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 2.000
R-factor	0.178
RMSD bond length	0.018 *
RMSD bond angle	3.030 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.050 *
Total number of observations	44352 *
Number of reflections	9759
Completeness [%]	81.0
Redundancy	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	25 (mg/ml)
2	1	2	ammonium sulfate	3.2 (M)
3	1	2	Tris-HCl	0.05 (M)