1LGV

Structure of a Human Bence-Jones Dimer Crystallized in U.S. Space Shuttle Mission STS-95: 100K

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU300
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	2001-01-18
Detector	MARRESEARCH
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	48.339, 83.248, 112.238
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 * - 1.950
Rwork	0.200
R-free	0.24500
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1jvk
RMSD bond length	0.016
RMSD bond angle	1.950 *
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.020
High resolution limit [Å]	1.950	1.950
Rmerge	0.047	0.450 *
Total number of observations	192398 *
Number of reflections	33875 *	3328 *
<I/σ(I)>	36.14	2.14
Completeness [%]	99.7	99.9
Redundancy	5.7	4.3 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *		279	Alvarado, U.R., (2001) J. Crystal Growth, 223, 407. *