1LFZ

OXY HEMOGLOBIN (25% METHANOL)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	298
Detector technology	IMAGE PLATE
Detector	RIGAKU
Spacegroup name	P 41 21 2
Unit cell lengths	52.800, 52.800, 192.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 3.100
R-factor	0.2
Rwork	0.200
R-free	0.26800
RMSD bond length	0.009
RMSD bond angle	1.400
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	CNS (0.4)

Data quality characteristics

	Overall
High resolution limit [Å]	3.100
Number of reflections	4267

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIQUID DIFFUSION	6.7	298	phosphate buffer, pH 6.7, LIQUID DIFFUSION at 298K