1LFV

OXY HEMOGLOBIN (88% RELATIVE HUMIDITY)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	298
Detector technology	IMAGE PLATE
Detector	RIGAKU
Wavelength(s)	1.5418
Spacegroup name	P 41 21 2
Unit cell lengths	54.200, 54.200, 194.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.800
R-factor	0.21
Rwork	0.210
R-free	0.27000
RMSD bond length	0.008
RMSD bond angle	1.300
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	CNS (0.4)

Data quality characteristics

	Overall
High resolution limit [Å]	2.800
Number of reflections	6350

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIQUID DIFFUSION	6.7	298	phosphate buffer, pH 6.7, LIQUID DIFFUSION at 298K