1LFB

THE X-RAY STRUCTURE OF AN ATYPICAL HOMEODOMAIN PRESENT IN THE RAT LIVER TRANSCRIPTION FACTOR LFB1(SLASH)HNF1 AND IMPLICATIONS FOR DNA BINDING

Experimental procedure

Spacegroup name	P 61 2 2
Unit cell lengths	81.030, 81.030, 85.180
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.000 - 2.800
R-factor	0.212
Rwork	0.212
R-free	0.36400
RMSD bond length	0.013
RMSD bond angle	3.360
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.800 *
Number of reflections	4344 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	acetate	100 (mM)
2	1	reservoir	ammonium sulfate	42 (%)