1LBI
LAC REPRESSOR
Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1996-01-01 |
| Detector | SIEMENS |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 160.300, 73.300, 147.800 |
| Unit cell angles | 90.00, 120.30, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.700 |
| R-factor | 0.25 |
| Rwork | 0.250 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 2.100 |
| Data reduction software | XDS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Rmerge | 0.072 |
| Number of reflections | 37143 |
| Completeness [%] | 89.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | macro seeding * | 8.5 * | 22 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG3000 | 32 (%) | |
| 2 | 1 | drop | potassium phosphate | 0.05 (M) | |
| 3 | 1 | drop | sodium potassium tartrate | 0.075 (M) | |
| 4 | 1 | drop | protein | 0.055 (mM) | |
| 5 | 1 | drop | DNA | 0.194 (mM) | |
| 6 | 1 | reservoir | PEG3000 | 29-31 (%) | |
| 7 | 1 | reservoir | potassium phosphate | 0.05 (M) | |
| 8 | 1 | reservoir | sodium potassium tartrate | 0.075 (M) |
