1KPF
PKCI-SUBSTRATE ANALOG
Experimental procedure
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1996-06-01 |
Detector | RIGAKU |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 40.150, 40.150, 143.190 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.500 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.24000 |
RMSD bond length | 0.020 |
RMSD bond angle | 24.801 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.062 | |
Total number of observations | 158000 * | |
Number of reflections | 36893 | |
Completeness [%] | 84.5 | |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.5 | 20 * | Lima, C.D., (1996) Proc.Nat.Acad.Sci.USA, 93, 5357. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 13-18 (%) | |
2 | 1 | reservoir | sodium cacodylate | 100 (mM) | |
3 | 1 | drop | PKCI-1 | 3-6 (mg/ml) |