1KIP

FV MUTANT Y(B 32)A (VH DOMAIN) OF MOUSE MONOCLONAL ANTIBODY D1.3 COMPLEXED WITH HEN EGG WHITE LYSOZYME

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1994-10-05
Detector	SIEMENS
Spacegroup name	C 1 2 1
Unit cell lengths	129.230, 60.440, 56.630
Unit cell angles	90.00, 119.05, 90.00

Refinement procedure

Resolution	7.000 - 2.100
R-factor	0.162
Rwork	0.162
RMSD bond length	0.015
RMSD bond angle	1.900
Data reduction software	XENGEN
Data scaling software	XENGEN
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Rmerge	0.086
Total number of observations	49442 *
Number of reflections	20023
Completeness [%]	91.3
Redundancy	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *			used to seeding *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	15-18 (%(w/v))
2	1	reservoir	potassium phosphate	0.1 (M)