1JYC
CONCANAVALIN A/15-mer PEPTIDE COMPLEX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54178 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 103.113, 118.547, 254.994 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.750 |
| Rwork | 0.195 |
| R-free | 0.24000 |
| Starting model (for MR) | 5cna |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS (0.5) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.750 |
| Rmerge | 0.100 |
| <I/σ(I)> | 6.2 |
| Completeness [%] | 78.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
