1JXX

CRAMBIN MIXED SEQUENCE FORM AT 200 K. PROTEIN/WATER SUBSTATES

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	200
Detector technology	DIFFRACTOMETER
Collection date	1990-12-17
Detector	RIGAKU AFC-5R
Spacegroup name	P 1 21 1
Unit cell lengths	40.870, 18.480, 22.370
Unit cell angles	90.00, 90.59, 90.00

Refinement procedure

Resolution	17.670 - 0.890
R-factor	0.136
Rwork	0.136
Starting model (for MR)	1jxw CRAMBIN MIXED FORM AT 180 K.
RMSD bond length	0.012
RMSD bond angle	0.033
Data reduction software	TEXSAN
Data scaling software	TEXSAN
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	17.670	0.910
High resolution limit [Å]	0.890	0.890
Rmerge	0.072 *
Number of reflections	26625
<I/σ(I)>	9.3	2.4
Completeness [%]	92.5	69
Redundancy	1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7	293	ethanol, pH 7.00, VAPOR DIFFUSION, SITTING DROP, temperature 293K