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STRUCTURE OF AVIAN H5 HAEMAGGLUTININ COMPLEXED WITH LSTA RECEPTRO ANALOG

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 14-BM-C
Synchrotron site	APS
Beamline	14-BM-C
Temperature [K]	100
Detector technology	CCD
Collection date	1999-12-31
Detector	ADSC QUANTUM 4
Wavelength(s)	1
Spacegroup name	H 3 2
Unit cell lengths	131.626, 131.626, 254.110
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.000 - 2.400
R-factor	0.24
Rwork	0.240
R-free	0.29600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009 *
RMSD bond angle	1.500 *
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	40.000
High resolution limit [Å]	2.400	2.400
Rmerge	0.106 *	0.709 *
Number of reflections	30623 *
Completeness [%]	92.7 *	94 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.5	298	mme-peg 2000, nicl2, hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K