1JP6
Sperm Whale met-Myoglobin (room temperature; room pressure)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 295 |
| Detector technology | AREA DETECTOR |
| Collection date | 1997-09-08 |
| Detector | UCSD MARK II |
| Wavelength(s) | 1.541 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.450, 30.930, 34.730 |
| Unit cell angles | 90.00, 105.73, 90.00 |
Refinement procedure
| Resolution | 9.200 * - 2.300 |
| R-factor | 0.16 * |
| Rwork | 0.162 |
| R-free | 0.21700 * |
| Starting model (for MR) | 1vxh |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.021 * |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 9.200 | 2.420 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.044 | 0.056 |
| Number of reflections | 5870 | |
| <I/σ(I)> | 14.7 | 15.6 |
| Completeness [%] | 96.9 | 94.5 |
| Redundancy | 2.6 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Batch method * | 6 | 298 | ammonium sulfate, pH 6, batch, temperature 298K |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ammonium sulfate | 72-78 (%sat) | pH5.5-6.0 |
