1JOD

Crystal Structure of Murine Olfactory Marker Protein in Spacegroup P43212

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X12C
Synchrotron site	NSLS
Beamline	X12C
Temperature [K]	130
Detector technology	CCD
Collection date	2000-04-15
Detector	CUSTOM-MADE
Wavelength(s)	0.9785
Spacegroup name	P 43 21 2
Unit cell lengths	89.128, 89.128, 158.982
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 3.200
R-factor	0.256
Rwork	0.256
R-free	0.32600
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	PDB ID 1F15
RMSD bond length	0.012
RMSD bond angle	1.800
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	X-PLOR (3.851)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	3.310
High resolution limit [Å]	3.200	3.200
Number of reflections	8962
Completeness [%]	80.4	61.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5	295	unpublished structure *