1IZA

ROLE OF B13 GLU IN INSULIN ASSEMBLY: THE HEXAMER STRUCTURE OF RECOMBINANT MUTANT (B13 GLU-> GLN) INSULIN

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	80.600, 80.600, 37.600
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	? - 2.500
R-factor	0.154
RMSD bond length	0.019
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.050 *
Number of reflections	3036 *
Completeness [%]	96.4 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	ammonium sulfate	1 (%(w/v))
2	1	reservoir	ammonium sulfate	4 (%(w/v))