Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1IWW

Crystal Structure Analysis of Human lysozyme at 152K.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]152
Detector technologyIMAGE PLATE
DetectorRIGAKU RAXIS IV
Spacegroup nameP 21 21 21
Unit cell lengths56.286, 61.121, 33.099
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution8.000 - 1.400
Rwork0.168
R-free0.19000
RMSD bond length0.011
RMSD bond angle1.300
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareNMREF
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.000
High resolution limit [Å]1.3501.350

*

Rmerge0.052

*

0.172

*

Total number of observations359305

*

Number of reflections24825
Completeness [%]96.2

*

60.7

*

Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.510

*

Takano, K., (1995) J. Mol. Biol., 254, 62.

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein10 (mg/ml)
21reservoir2.5 (M)
31reservoiracetate20 (mM)

219869

PDB entries from 2024-05-15

PDB statisticsPDBj update infoContact PDBjnumon