1IQF
Human coagulation factor Xa in complex with M55165
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-02-18 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 72.290, 78.040, 56.630 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 3.200 |
| Rwork | 0.169 |
| R-free | 0.27700 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.400 |
| Phasing software | GLRF |
| Refinement software | CNX (2000) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 3.300 | |
| High resolution limit [Å] | 3.200 | 3.200 |
| Rmerge | 0.053 | 0.071 |
| Number of reflections | 4578 | |
| Completeness [%] | 80.8 | 66.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.2 | 293 | PEG1500, calcium chloride, M55165, tris-HCl, pH 7.2, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
