1INF
INFLUENZA VIRUS B/LEE/40 NEURAMINIDASE COMPLEXED WITH BANA113 INHIBITOR
Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1994-04-22 |
| Detector | SIEMENS |
| Spacegroup name | P 4 21 2 |
| Unit cell lengths | 124.250, 124.250, 71.350 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.500 - 2.400 |
| R-factor | 0.159 |
| Rwork | 0.159 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.920 |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.900 * |
| Rmerge | 0.125 |
| Number of reflections | 17683 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.4 | Lin, Y., (1990) J. Mol. Biol., 214, 639. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG4000 | 15 (%(v/v)) | |
| 2 | 1 | drop | HEPES | 0.01 (M) | pH7.4 |
| 3 | 1 | drop | 10 (mM) | ||
| 4 | 1 | drop | 2.5 (mM) | ||
| 5 | 1 | reservoir | PEG4000 | 30 (%(v/v)) | |
| 6 | 1 | reservoir | HEPES | 0.02 (M) | pH7.4 |
