1ICJ

PDF PROTEIN IS CRYSTALLIZED AS NI2+ CONTAINING FORM, COCRYSTALLIZED WITH INHIBITOR POLYETHYLENE GLYCOL (PEG)

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	140.700, 63.400, 86.900
Unit cell angles	90.00, 120.60, 90.00

Refinement procedure

Resolution	6.000 - 1.900
R-factor	0.198
Rwork	0.198
R-free	0.23000
RMSD bond length	0.010
RMSD bond angle	25.200 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.900 *	1.900 *
Rmerge	0.075 *	0.247 *
Completeness [%]	97.9 *	95.3 *
Redundancy	5.5 *	2.1 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	2 (M)
2	1	1	PEG1000	1 (%(w/v))