1IBE
DEOXY-HAEMOGLOBIN TRAPPED IN THE HIGH-AFFINITY (R) STATE
Experimental procedure
| Detector technology | AREA DETECTOR |
| Detector | XUONG-HAMLIN MULTIWIRE |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 108.180, 63.180, 54.580 |
| Unit cell angles | 90.00, 111.10, 90.00 |
Refinement procedure
| Resolution | ? - 1.800 |
| R-factor | 0.1786 * |
| Rwork | 0.179 |
| R-free | 0.23000 |
| RMSD bond length | 0.024 |
| RMSD bond angle | 0.044 |
| Data reduction software | UCSD |
| Data scaling software | UCSD |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.800 * |
| Rmerge | 0.059 |
| Total number of observations | 144335 * |
| Number of reflections | 32227 |
| Completeness [%] | 98.1 |
| Redundancy | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Batch method * | 6.4 * | Perutz, M.F., (1968) J. Crystal Growth, 2, 54. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | phosphate | 3.4 (M) | |
| 2 | 1 | 1 | potassium phosphate | 0.45vol | |
| 3 | 1 | 1 | sodium phosphate | 0.55vol | |
| 4 | 1 | 1 | 0.18vol |
