1IAG

FIRST STRUCTURE OF A SNAKE VENOM METALLOPROTEINASE: A PROTOTYPE FOR MATRIX METALLOPROTEINASES(SLASH)COLLAGENASES

Experimental procedure

Spacegroup name	P 32 1 2
Unit cell lengths	73.600, 73.600, 96.400
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 2.000
R-factor	0.172
Rwork	0.172
RMSD bond length	0.016
RMSD bond angle	1.900
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.000 *	2.030 *
Rmerge	0.054 *
Total number of observations	24244 *
Number of reflections	17021 *
Completeness [%]	83.0 *	42 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	1.8 (M)