1HXN

1.8 ANGSTROMS CRYSTAL STRUCTURE OF THE C-TERMINAL DOMAIN OF RABBIT SERUM HEMOPEXIN

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	43.600, 62.800, 80.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.800
R-factor	0.176
RMSD bond length	0.014
RMSD bond angle	1.200
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.040 *
Total number of observations	51808 *
Number of reflections	16990 *
Completeness [%]	81.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5.25 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	6 (mg/ml)
2	1	drop	sodium citrate	0.1 (M)
3	1	drop	ammonium acetate	0.3 (M)
4	1	drop	methoxypolyethylene glycol1500	20 (%(w/v))