1HV7

PORCINE PANCREATIC ELASTASE COMPLEXED WITH GW311616A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1998-03-19
Detector	RIGAKU RAXIS II
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	49.568, 58.327, 74.054
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.700
R-factor	0.1523
Rwork	0.150
R-free	0.20070
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.013
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	29.111
High resolution limit [Å]	1.700
Rmerge	0.051
Number of reflections	24111
Completeness [%]	99.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	4.6	293	PEG4000, ammonium sulphate, sodium acetate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K