1HRV

HRV14/SDZ 35-682 COMPLEX

Experimental procedure

Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Detector technology	FILM
Collection date	1990-06
Spacegroup name	P 21 3
Unit cell lengths	445.100, 445.100, 445.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 3.000
Data reduction software	PURDUE (DATA PROCESSING PACKAGE)
Refinement software	REFI (IN O)

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	3.000 *
Rmerge	0.123
Total number of observations	78617 *
Number of reflections	60785 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.2 *		3-4 CRYSTALS SOAKED IN 200 MICROLITER DROPS OF SDZ 35-682 (5 MICROGRAM/ML).
1	Vapor diffusion, hanging drop *	7.2 *		3-4 CRYSTALS SOAKED IN 200 MICROLITER DROPS OF SDZ 35-682 (5 MICROGRAM/ML).

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	0.005 (mg/ml)
2	1	drop	Tris-HCl	10 (mM)
3	1	drop	PEG8000	0.25-0.75 (%(w/v))