1HRI

STRUCTURE DETERMINATION OF ANTIVIRAL COMPOUND SCH 38057 COMPLEXED WITH HUMAN RHINOVIRUS 14

Experimental procedure

Spacegroup name	P 21 3
Unit cell lengths	445.100, 445.100, 445.100
Unit cell angles	90.00, 90.00, 90.00

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000 *
High resolution limit [Å]	3.000 *	3.000 *
Rmerge	0.120 *
Number of reflections	147740 *	40195 *
Completeness [%]		19 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.2 *		taken from Arnold, E. et al (1984). J. Mol. Biol., 177, 417-430. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	Tris-HCl	0.01 (M)
2	1	drop	PEG8000	0.25-0.75 (%(w/v))
3	1	drop		0.01 (M)
4	1	drop	protein	5 (mg/ml)
5	1	reservoir	PEG8000	0.25-0.5 (%(w/v))
6	1	reservoir		0.02 (M)
7	1	reservoir	Tris-HCl	0.01 (M)