1HHF
Decaplanin second P6122-Form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7B |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-09-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 60.101, 60.101, 131.387 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.390 - 1.470 |
| R-factor | 0.18 |
| R-free | 0.21110 |
| Structure solution method | OTHER |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.027 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHELXD |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.390 | 1.600 |
| High resolution limit [Å] | 1.470 | 1.470 |
| Rmerge | 0.051 | 0.350 |
| Number of reflections | 24558 | |
| <I/σ(I)> | 18.74 | 5.96 |
| Completeness [%] | 99.1 | 99.6 |
| Redundancy | 12 | 11 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 0.1M TRIS/HCL, PH=8.5, 2M NH4H2PO4, pH 8.50 |
