1HEW

REFINEMENT OF AN ENZYME COMPLEX WITH INHIBITOR BOUND AT PARTIAL OCCUPANCY. HEN EGG-WHITE LYSOZYME AND TRI-N-ACETYLCHITOTRIOSE AT 1.75 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	78.860, 78.860, 38.250
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 1.750
R-factor	0.229
RMSD bond length	0.021
RMSD bond angle	0.032 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.750 *
Rmerge	0.057 *
Total number of observations	18180 *
Number of reflections	12579 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *	4.7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	lysozyme	40 (mg/ml)
2	1	1		5 (%(w/v))
3	1	1	acetate	0.04 (M)
4	1	1	(GlcNAc)3	8.9 (mg/ml)
5	1	1	inhibitor