1HC0
structure of lysozyme with periodate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR591 |
| Temperature [K] | 150 |
| Detector technology | IMAGE PLATE |
| Detector | MAR scanner 345 mm plate |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 77.765, 77.765, 37.555 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.820 |
| Structure solution method | AB INITIO PHASING |
| Data reduction software | HKL1998 |
| Data scaling software | HKL (V. 1998) |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 25.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 13140 |
| <I/σ(I)> | 5.9 |
| Completeness [%] | 70.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.5 | SOAKED AT PERIODATE, pH 4.50 |
