1HAB

CROSSLINKED HAEMOGLOBIN

Experimental procedure

Source type	ROTATING ANODE
Source details	RIGAKU RUH2R
Temperature [K]	298
Detector technology	AREA DETECTOR
Detector	ADSC
Spacegroup name	P 21 21 21
Unit cell lengths	86.840, 87.110, 97.630
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 2.300
R-factor	0.191 *
Rwork	0.191
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.017
RMSD bond angle	1.949
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.300 *
Rmerge	0.056 *
Total number of observations	105634 *
Number of reflections	34416
Completeness [%]	99.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *	6.7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	sodium potassium phosphate	2.4 (M)