1GRI
GRB2
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | LURE BEAMLINE DW32 |
| Synchrotron site | LURE |
| Beamline | DW32 |
| Detector technology | IMAGE PLATE |
| Collection date | 1994-07 |
| Detector | MARRESEARCH |
| Spacegroup name | P 43 |
| Unit cell lengths | 88.870, 88.870, 97.960 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 3.100 |
| R-factor | 0.213 |
| Rwork | 0.213 |
| RMSD bond length | 0.022 |
| RMSD bond angle | 28.810 * |
| Data reduction software | MOSFLM (V. 5.21) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Rmerge | 0.087 |
| Number of reflections | 14079 |
| Completeness [%] | 92.4 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Microdialysis * | 8 * | 19 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | protein | 15 (mg/ml) | |
| 2 | 1 | 2 | sodium acetate |
