Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Detector | MULTIWIRE XENTRONICS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.039, 68.302, 41.440 |
| Unit cell angles | 90.00, 113.87, 90.00 |
Refinement procedure
| Resolution | 33.300 - 1.920 |
| R-factor | 0.147 |
| Rwork | 0.147 |
| R-free | 0.19100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2exo |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.480 |
| Data reduction software | XENGEN |
| Data scaling software | XENGEN |
| Phasing software | AMoRE |
| Refinement software | CNS (0.9) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.330 | 2.050 |
| High resolution limit [Å] | 1.920 | 1.920 |
| Rmerge | 0.071 | 0.160 |
| Number of reflections | 15469 | |
| Completeness [%] | 81.6 | 35 |
| Redundancy | 4.4 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | HANGING DROPS CONTAINING 1:1 RATIO OF 20 MG/ML PROTEIN SOLUTION AND RESERVOIR SOLUTION (12 % TO 25 % PEG 6,000)., pH 7.00 |
